| 其它标识： |
MDL：MFCD00238543
SMILES：O=C1C(C)=C(C[C@@]23[H])[C@@](C[C@@]3(C)CCCC2=C)(O)O1
InChI：InChI=1S/C15H20O3/c1-9-5-4-6-14(3)8-15(17)12(7-11(9)14)10(2)13(16)18-15/h11，17H，1，4-8H2，2-3H3/t11-，14+，15-/m0/s1
Note：储备液建议分装冻存,避免反复冻融(-20℃,1个月);稀释后的工作液建议现用现配
|
| 基本信息： |
CAS：73030-71-4
中文名称：白术内酯III
英文名称：Atractylenolide Ⅲ
别名：8β-Hydroxyasterolide;ICodonolactone
纯度：HPLC≥98%
分子式：C15H20O3
分子量：248.32
外观(性状)：白色至类白色结晶或粉末
规格：20mg
溶解性：≥10mg/mL in DMSO
储存条件：Store at 2-8℃，2 years.
|
| 溶解性： |
≥10mg/mL in DMSO |
产品详情
本品为分析标准品。
使用本产品的案例（仅供参考）
UPLC-PDA
The levels of the main active ingredients of MSJZT were detected using a UPLC-PDA method. Chromatographic separation was performed on a UPLC system with a photodiode array detector (PDA) and C18 (100 mm×2.1 mm, 1.7μm ) column. The column temperature was set at 30℃. The mobile phase was composed of 0.1% phosphoric acid (A) and acetonitrile (B). The optimum adsorption and elution conditions were set as follows: 0–1.5 min, 95% B; 1.5–6 min, 95–80% B; 7–10 min, 80–60% B; 10–10.5 min, 50–35% B; 10.5–12 min, 35–30% B; 12–12.5 min, 30–20% B; 12.5–16 min, 20–10% B; 16–16.5 min, 10–0% B; and 16.5–18 min, 0–95% B.
来源文献：Nie S, Zhao Y, Qiu X, Wang W, Yao Y, Yi M, Wang D. Metabolomic Study on Nude Mice Models of Gastric Cancer Treated with Modified Si Jun Zi Tang via HILIC UHPLC-Q-TOF/MS Analysis. Evid Based Complement Alternat Med. 2019 Jun 23;2019:3817879. doi: 10.1155/2019/3817879. PMID: 31341492; PMCID: PMC6612382.
HPLC
The active components of ZZD were analyzed by LC AT-20 HPLC with double solvent pump high-pressure gradient system and SPD-20A photodiode array detector. The chromatography was performed on 5 lm particles, 250 × 4.6 mm, C18 column (35 ℃) at a flow rate of 1.0 mL/min and eluted with 0.1% formic acid aqueous solution (A) and 0.1% formic acid acetonitrile (B), and the gradient elution was 0–7 min, 23% B; 7–17 min, 23–80% B; 17–20 min, 80–100% B; 20–30 min, 100% B.
来源文献：Wen Y, Zhan Y, Tang S, Liu F, Wu R, Kong P, Li Q, Tang X. Zhizhu decoction alleviates slow transit constipation by regulating aryl hydrocarbon receptor through gut microbiota. Pharm Biol. 2023 Dec;61(1):111-124. doi: 10.1080/13880209.2022.2157020. Erratum in: Pharm Biol. 2023 Dec;61(1):1413. PMID: 36562308; PMCID: PMC9793913.
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